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小尺寸水泥净浆断裂韧性测试参数优化与精度评价

Optimization of Fracture Toughness Testing Method for Small-sized Cement Paste Specimens

  • 摘要: 在水泥基材料研究中,浆体作为关键胶凝组分,其性能对材料宏观行为具有决定性影响。当涉及特殊添加剂或需精确控制原材料级配时,传统大尺寸试件因原料消耗大、制备效率低,难以满足快速研发需求。针对这一瓶颈,本文开发了小尺寸水泥净浆断裂韧性精确测试方法。通过系统研究预制裂缝深度、加载跨距及速率等参数的影响规律,建立了优化测试方案。研究采用精密三点弯曲试验装置,重点解决了小尺寸试件断裂路径随机性大的技术难题。通过对荷载-位移曲线进行分段线性化处理,显著提升了测试可靠性。试验结果表明,当预制裂缝深度为试件厚度的35%、跨距为100 mm、加载速率为0.1 mm/min时,断裂韧性、断裂能的测试变异系数可控制在2%和4%以内。与传统方法相比,本方法将试件尺寸减小约70%,大幅降低原料用量,为特殊配比材料的快速性能评估提供了有效手段。该方法在新材料研发和特种工程材料性能评价中具有重要应用价值,为推动水泥基材料精细化设计提供了新的技术途径。

     

    Abstract: In the study of cement-based materials, cement paste plays a decisive role in determining macroscopic material behavior. However, traditional large specimens face challenges such as high material consumption and low preparation efficiency when special additives or precise gradation control is required. To address this, an accurate fracture toughness test for small-sized cement paste specimens was developed. By systematically investigating the effects of pre-crack depth, support span, and loading rate, an optimized testing protocol was established using a precision three-point bending setup. Key issues such as randomness in fracture paths were resolved through segmented linear processing of load-displacement curves, significantly improving reliability. Results show that with a pre-crack depth of 35% of specimen thickness, a span of 100 mm, and a loading rate of 0.1 mm/min, the coefficients of variation for fracture toughness and fracture energy are within 2%/4%. Compared to conventional methods, this approach reduces specimen size by about 70%, greatly lowers material consumption, and provides an effective means for rapid performance evaluation of specially proportioned materials. It offers valuable application in new material development and performance assessment of specialty engineering materials, supporting the refined design of cement-based materials.

     

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